Multi-wall carbon nanotubes, MWNT, single-wall carbon nanotube, SWNT and
aligned multi-wall carbon nanotubes, AMWNT can be synthesized
by Chemical Vapor Deposition (CVD) method. Two hybrids of this technique are involved
in the growth study of cabon nanotubes: thermal-CVD and plasma-CVD.
Thermal - chemical vapor deposition
A thermal-CVD system was built for carbon nanotubes production via gas phase
or on substrate surface. The skech of thermal-CVD system consists of quartz
tube furnace which can operate till 1200 degreecentigrades. The sketch of our
equipment is shown in figure 1. Main advantages of
a thermal-CVD are: the absolute ability for mass production of nanotubes
material and the controllable growth of carbon nanotubes at a specific location
on a substrate for incorporation in electronic device.
Figure 1: Thermal-CVD experimental set-up
Plasma Enhanced - chemical vapor deposition
A controllable method for cabon nanotubes production is plasma enhanced-CVD.
Such a system is often used to grow free standing vertically aligned MWCNT. The
set-up which our laboratory is equipt with is a glow discharged type. Briefly, two
electrodes are placed in a steinless-steel chamber. The grounded cathode plays the role
of a substrate holder and Ohmic heater. On the anod is applied aprox.400V.
Figure 2: Plasma-CVD experimental set-up